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1 article(s) from Peptu, Cristian

Cyclodextrins tethered with oligolactides – green synthesis and structural assessment

Cristian Peptu,
Mihaela Balan-Porcarasu,
Alena Šišková,
Ľudovít Škultéty and
Jaroslav Mosnáček

Beilstein J. Org. Chem. 2017, 13, 779–792, doi:10.3762/bjoc.13.77

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Graphical Abstract

Scheme 1: Ring opening of L-LA in the presence of cyclodextrins.

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Figure 1: (a) ELSD chromatogram of crude β-CD-LA reaction mixture and (b) MALDI–MS spectrum of fraction f5.

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Figure 2: MALDI–MS spectra of the fractionated α-, β- and γ-CD-LA products – fractions precipitated in THF: (...

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Figure 3: MALDI–MS spectra of the fractionated α-, β- and γ-CD-LA products – fractions soluble in THF: (a) α-...

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Figure 4: ¹H NMR spectrum of fractions precipitated in THF of (A) α-CD-LA, (B) β-CD-LA and (C) γ-CD-LA.

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Figure 5: ¹³C NMR spectra of (A) β-CD-LA F2 fraction and (B) β-CD-LA F1 fraction.

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Figure 6: DEPT135-NMR experiment of (A) β-CD-LA F2 fraction and (B) β-CD-LA F1 fraction.

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Published 26 Apr 2017

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